mgco3 ra mgo

  • Bin Zhang7,8,
  • Jinhui Peng8,
  • Libo Zhang8 &
  • Shaohua Ju8 
  • Chapter


The conditions of technique vĩ đại prepare magnesium oxide by calcination from basic magnesium carbonate were optimized using a central composite design (CCD) of response surface methodology (RSM). Two quadratic equation models for decomposition rate and activity of magnesium oxide were built and effects of main factors and their corresponding relationships were obtained. The statistical analysis of the results showed that in the range studied the decomposition rate and activity of magnesium oxide were significantly affected by the calcination temperature and calcination time. The optimized calcination conditions were as follows: the calcination temperature 666.99°C and the calcination time 2.12 h, respectively. Under these conditions the decomposition rate of basic magnesium carbonate was 92.1971%, and the activity of magnesium oxide was 155.503 mg I2/g MgO. The validity of the model was confirmed experimentally and the results were satisfactory. In addition, the sample was characterized by X-ray Diffraction (XRD).


  • Response surface methodology
  • Basic magnesium carbonate
  • Calcination
  • Magnesium oxide


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  1. W.J. Climent, A. Corma, S. Iborra, M. Mifsud. MgO nanoparticle-based multifunctional catalysts in the cascade reaction allows the green synthesis of anti-inflammatory agents [J]. J. Catal, 2007, 247:223–230

  2. Fereshteh Meshkani, Mehran Rezaei. Effect of process parameters on the synthesis of nanocrystalline magnesium oxide with high surface area and plate-like shape by surfactant assisted precipitation method [J]. Powder Technology, 2010, 199:144–148

  3. I.V. Mishakov, A.F. Bedilo, R.M. Richards, V.V. Chesnokov, A.M. Volodin, V.I. Zaikovskii, R.A. Buyanov, K.J. Klabunde. Nanocrystalline MgO as a dehydrohalogenation catalyst [J]. J. Catal. 2002, 206:40–48

  4. V.V. Chesnokov, A.F. Bedilo, D.S. Heroux, I.V. Mishakov, K.J. Klabunde, Oxidative dehydrogenation of butane over nanocrystalline MgO, Al2O3, and VOx/MgO catalysts in the presence of small amounts of iodine [J]. J. Catal., 2003, 218:438–446

  5. N. Takahashi. Simple and rapid synthesis of MgO with nano-cube shape by means of a domestic microwave oven [J]. Solid State Sciences, 2007, 9:722–724

  6. Bingguo Liu, Jinhui Peng, Libo Zhang, Rundong Wan, Shenghui Guo, Liexing Zhou. Optimization of preparation for Co3O4 by calcination from cobalt oxalate using response surface methodology [J]. Chemical Engineering Research and Design, 2010, 88(8):971–976

  7. Ming-Ju Chen, Kun-Nan Chen, Chin-Wen Lin. Optimization on response surface models for the optimal manufacturing conditions of dairy tofu [J]. Journal of Food Engineering, 2005, 68(4):471–480

  8. Jianfeng Fu, Yaqian Zhao, Qiuli Wu. Optimising photoelectrocatalytic oxidation of fulvic acid using response surface methodology [J]. Journal of Hazardous Materials, 2007, 144(1–2):499–505

  9. Bala Kiran, Anubha Kaushik, C.P. Kaushik. Response surface methodological approach for optimizing removal of Cr(VI) from aqueous solution using immobilized cyanobacterium [J]. Chemical Engineering Journal, 2007, 126(2–3):147–153

  10. Sarayu Mohana, Shalini Shrivastava, Jyoti Divecha, Datta Madamwar. Response surface methodology for optimization of medium for decolorization of textile dye Direct Black 22 by a novel bacterial consortium [J]. Bioresource Technology, 2008, 99(3):562–569

  11. R. Azargohar, A.K. Dalai. Production of activated carbon from Luscar char: Experimental and modeling studies [J]. Microporous and Mesoporous Materials, 2005, 85(3):219–225

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  12. A.L. Ahmad, S.C. Low, S.R. Abd Shukor, A. Ismail. Optimization of membrane performance by thermal-mechanical stretching process using responses surface methodology (RSM) [J]. Separation and Purification Technology, 2009, 66(1):177–186

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Authors and Affiliations

  1. Kunming University of Science and Technology, Kunming Yunnan, 650093, quảng cáo China

    Bin Zhang (Faculty of Science)

  2. Faculty of Metallurgy and Energy Engineering, Kunming University of Science and Technology, Kunming Yunnan, 650093, quảng cáo China

    Bin Zhang (Faculty of Science), Jinhui Peng, Libo Zhang & Shaohua Ju

Editor information

Editors and Affiliations

  1. Department of Materials Science and Engineering, North Carolina State University, USA

    Suveen N. Mathaudhu (Adjunct Assistant Professor) (Adjunct Assistant Professor)

  2. Netherlands Organization for Applied Scientific Research (TNO), Netherlands

    Wim H. Sillekens (Senior Scientist) (Senior Scientist)


    Neale R. Neelameggham (Guru) (Guru)

  4. Magnesium Processing Department at the Magnesium Innovation Centre (MagIC), Helmholtz-Zentrum Geesthacht Zentrum für Material- und Küstenforschung, Geesthacht, Germany

    Norbert Hort (head) (head)

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Zhang, B., Peng, J., Zhang, L., Ju, S. (2012). Optimization of Preparation for Magnesium Oxide by Calcination from Basic Magnesium Carbonate Using Response Surface Methodology. In: Mathaudhu, S.N., Sillekens, W.H., Neelameggham, N.R., Hort, N. (eds) Magnesium Technology 2012. Springer, Cham.

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  • Print ISBN: 978-3-319-48571-3

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