h3po4 ra co2

Abstract

The preparation of activated carbon from rice husk residue using H3PO4 as activation agent was studied. The samples were characterized by elemental analysis, N2 adsorption–desorption, scanning electron microscopy (SEM), X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), temperature programmed decomposition-mass spectra (TPD-MS), thermogravimetric analysis (TGA) and X-ray photoelectron spectroscopy (XPS). The role of H3PO4 in the activation process was discussed. A maximum surface area of 1016 m2 g−1 was obtained under the optimized conditions, that is, a base treated solid material to tướng H3PO4 mass ratio of 1 : 2, an activation temperature of 500 °C and an activation time of 1 h. H3PO4 might act as a catalyst which facilitates the release of CO2, an oxidant which reacts with carbon after dehydration, and a reagent which enters AC through C–O–P bonds.

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Graphical abstract: The role of H3PO4 in the preparation of activated carbon from NaOH-treated rice husk residue

Article information

DOI
https://doi.org/10.1039/C5RA04634C

Article type
Paper

Submitted
16 Mar 2015

Accepted
31 Mar 2015

First published
31 Mar 2015

RSC Adv., năm ngoái,5, 32626-32636

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The role of H3PO4 in the preparation of activated carbon from NaOH-treated rice husk residue

Y. Li, X. Zhang, R. Yang, G. Li and C. Hu, RSC Adv., năm ngoái, 5, 32626 DOI: 10.1039/C5RA04634C

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